Difference between revisions of "Talk:Fluorine Reaction"
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Nickel and Monel crucibles, using copper gaskets, are compatible with the fluorine gas. Teflon is appropriate for gaskets and tubing at lower temperatures. At higher temperatures, platinum crucibles would be needed, but the eutectic electrolysis should have a temperature low enough to that platinum isn't required. See J. Grannec and L. Lozano, "2: Preparative Methods", in the book Inorganic Solid Fluorides, P. Hagenmuller (ed.), Academic Press, NY, 1985, pp. 17-76. | Nickel and Monel crucibles, using copper gaskets, are compatible with the fluorine gas. Teflon is appropriate for gaskets and tubing at lower temperatures. At higher temperatures, platinum crucibles would be needed, but the eutectic electrolysis should have a temperature low enough to that platinum isn't required. See J. Grannec and L. Lozano, "2: Preparative Methods", in the book Inorganic Solid Fluorides, P. Hagenmuller (ed.), Academic Press, NY, 1985, pp. 17-76. | ||
[[User:Geoffrey.landis|Geoffrey.landis]] 07:23, 14 March 2007 (PDT) | [[User:Geoffrey.landis|Geoffrey.landis]] 07:23, 14 March 2007 (PDT) | ||
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| + | I have an Inter-Library Loan request pending for "Inorganic Solid Fluorides: Chemistry and Physics (Materials Science and Technology Series) (Hardcover)" by Paul Hagenmuller as of this date. Hopefully I will have it before ISDC. | ||
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| + | [[User:Jarogers2001|Jarogers2001]] 14:56, 9 May 2007 (UTC) | ||
Revision as of 06:56, 9 May 2007
How do you propose to mitigate flourine induced stress crack corrosion in your piping? Teflon can be used in some piping but has temperature limitations. Is there an inert refractory material that could be used as a crucible for the salt melt or a lining in the plasma reduction stage? -- Jarogers2001 21:15, 13 March 2007 (PDT)
Materials
Nickel and Monel crucibles, using copper gaskets, are compatible with the fluorine gas. Teflon is appropriate for gaskets and tubing at lower temperatures. At higher temperatures, platinum crucibles would be needed, but the eutectic electrolysis should have a temperature low enough to that platinum isn't required. See J. Grannec and L. Lozano, "2: Preparative Methods", in the book Inorganic Solid Fluorides, P. Hagenmuller (ed.), Academic Press, NY, 1985, pp. 17-76. Geoffrey.landis 07:23, 14 March 2007 (PDT)
I have an Inter-Library Loan request pending for "Inorganic Solid Fluorides: Chemistry and Physics (Materials Science and Technology Series) (Hardcover)" by Paul Hagenmuller as of this date. Hopefully I will have it before ISDC.
Jarogers2001 14:56, 9 May 2007 (UTC)
